HuagongsheHuagongshe Chemistry Print Report · For research reference only
1H-1,2,4-Triazole → 4-(3,4-Dimethoxyphenyl)-3-hexanoyl-6,7-dimethoxy-2-(1,2,4-triazol-1-ylmethyl)quinoline
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1H-1,2,4-Triazole | HCID 9257 | — |
| Reactant | 2-Bromomethyl-4-(3,4-dimethoxyphenyl)-3-hexanoyl-6,7-dimethoxyquinoline | HCID 19039898 | — |
| Product | 4-(3,4-Dimethoxyphenyl)-3-hexanoyl-6,7-dimethoxy-2-(1,2,4-triazol-1-ylmethyl)quinoline | HCID 19039895 | — |
Reaction Steps
According to the same manner as that described in Example 3, 2-bromomethyl-4-(3,4-dimethoxyphenyl)-3-hexanoyl-6,7-dimethoxyquinoline was reacted with 1H-1,2,4-triazole to give 4-(3,4-dimethoxyphenyl)-3-hexanoyl-6,7-dimethoxy-2-(1,2,4-triazol-1-ylmethyl)quinoline. This compound was recrystallized from ethanol to give colorless prisms. mp. 151°-152° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05641788 |
| Source dataset | uspto-grants-1997_06 |
| ORD ID | ord-d8af5a6003e0416a8a7c44b20b907373 |
| Source note | uspto-grants-1997_06 |