HuagongsheHuagongshe Chemistry Print Report · For research reference only
Formaldehyde → N-Methylolmaleimide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Formaldehyde | HCID 712 | — |
| Reactant | Sodium Carbonate | HCID 10340 | — |
| Reactant | Maleimide | HCID 10935 | — |
| Solvent | Water | HCID 962 | — |
| Product | N-Methylolmaleimide | HCID 227678 | 18,971.5% |
Reaction Steps
A mixture of 9.8 g (0.1 mole) maleimide, 9 ml 37% aqueous formaldehyde and 40 mg sodium carbonate was stirred at room temperature for 1 hour. The mixture was diluted with 30 ml water and the crystals formed (9.1 g N-hydroxymethylmaleimide) were collected by filtration.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05641856 |
| Source dataset | uspto-grants-1997_06 |
| ORD ID | ord-c327091779444e2f89fee3422e55da20 |
| Source note | uspto-grants-1997_06 |