HuagongsheHuagongshe Chemistry Print Report · For research reference only
(S)-(+)-1-Indanyl isocyanate → HCID 86628148, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (S)-(+)-1-Indanyl isocyanate | HCID 7018270 | — |
| Reactant | HCID 178426134 | HCID 178426134 | — |
| Solvent | tetrahydrofuran N,N-dimethylformamide | HCID 21974620 | — |
| Product | HCID 86628148 | HCID 86628148 | — |
Reaction Steps
In analogy to example 1c, 200 mg (1.089 mmol) of 6-chloro-4-methyl-1H-pyrazolo-[3,4-b]pyridin-3-ol were reacted with 208.1 mg (1.2 mmol) of (S)-1-isocyanatoindane in THF/DMF at RT. Yield: 153 mg (41%), M+H+: 343.32.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08148395B2 |
| Source dataset | uspto-grants-2012_04 |
| ORD ID | ord-276a8f36a8084bcbbc49604499094155 |
| Source note | uspto-grants-2012_04 |