HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Naphthalenesulfonyl chloride → HCID 9910511, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Naphthalenesulfonyl chloride | HCID 7125 | — |
| Reactant | Sodium bis(trimethylsilyl)amide | HCID 2724254 | — |
| Reactant | 3-(1,2,3,5,8,8a-hexahydro-7-indolizinyl)-1H-5-Azaindole | HCID 10130974 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 9910511 | HCID 9910511 | — |
Reaction Steps
3-(1,2,3,5,8,8a-hexahydro-7-indolizinyl)-1H-5-Azaindole (10 mg, 0.0418 mmol), 2-naphthalenesulfonyl chloride (20 mg, 0.088 mmol) and 1M NaN(TMS)2 (100 μL, 0.10 mmol) in THF (0.5 mL) at RT.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08148394B2 |
| Source dataset | uspto-grants-2012_04 |
| ORD ID | ord-e2175ab19100497cbec596b98c7caa4a |
| Source note | uspto-grants-2012_04 |