2-(Methylamino)ethanol → HCID 59200351, compound

HRID 1685310Notes

Reaction equation

HRID 1685310 reaction equation
[CH2:1]([N:3]([CH2:20]C)[CH2:4][C:5]([C:14]1[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=1)([C:8]1[CH:13]=[CH:12][CH:11]=[CH:10][CH:9]=1)[CH2:6][NH2:7])[CH3:2].CNCC[OH:26]>>[NH2:7][CH2:6][C:5]([C:14]1[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=1)([C:8]1[CH:13]=[CH:12][CH:11]=[CH:10][CH:9]=1)[CH2:4][N:3]([CH3:20])[CH2:1][CH2:2][OH:26]

Participants

3

Reactant 2

HCID 80162-(Methylamino)ethanolHCID 59200426N1,N1-diethyl-2,2-diphenylpropane-1,3-diamine

Product 1

HCID 59200351HCID 59200351, compound

Procedure

The title material was prepared as described for the synthesis of N1,N1-diethyl-2,2-diphenylpropane-1,3-diamine (Example Q) in using 2-(methylamino)ethanol. LC/MS (M+H)+: 285. HPLC ret. time (Condition B): 1.405 min.

Workup

  1. custom1.405 min.

Sources & evidence

ORD record
ord-9cd6809d55f24b75a912157d4d71d151
Source dataset
uspto-grants-2012_04
Patent number
US08148400B2

Reaction notes

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