(2-Methoxyethyl)(methyl)amine → HCID 59200487, compound
Reaction equation
[CH2:1]([N:3]([CH2:20]C)[CH2:4][C:5]([C:14]1[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=1)([C:8]1[CH:13]=[CH:12][CH:11]=[CH:10][CH:9]=1)[CH2:6][NH2:7])[CH3:2].[CH3:22][O:23]CCNC>>[CH3:22][O:23][CH2:2][CH2:1][N:3]([CH3:20])[CH2:4][C:5]([C:14]1[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=1)([C:8]1[CH:13]=[CH:12][CH:11]=[CH:10][CH:9]=1)[CH2:6][NH2:7]Participants
3
Procedure
The title material was prepared as described for the synthesis of N1,N1-diethyl-2,2-diphenylpropane-1,3-diamine (Example Q) in using 2-methoxy-N-methylethanamine LC/MS (M+H)+: 299. HPLC ret. time (Condition B): 1.480 min.
Workup
- custom1.480 min.
Sources & evidence
- ORD record
- ord-8ba13020e8c24ed7adca7b6d1f1c31b7
- Source dataset
- uspto-grants-2012_04
- Patent number
- US08148400B2
Reaction notes
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