HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Chloro-4-fluorobenzeneboronic acid → HCID 67291973, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Chloro-4-fluorobenzeneboronic acid | HCID 17750229 | — |
| Reactant | 5-bromo-3-pyridinyl 2,3,4-tri-O-acetyl-5-thio-beta-D-xylo-pyranoside | HCID 44195502 | — |
| Product | HCID 67291973 | HCID 67291973 | — |
Reaction Steps
By following a procedure analogous to Example 27 starting from 5-bromo-3-pyridinyl 2,3,4-tri-O-acetyl-5-thio-β-D-xylopyranoside and 2-chloro-4-fluoro-phenylboronic acid, 5-(2-chloro-4-fluorophenyl)-3-pyridinyl 2,3,4-tri-O-acetyl-5-thio-β-D-xylopyranoside is obtained in the form of an off-white foam (yield 81%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08148407B2 |
| Source dataset | uspto-grants-2012_04 |
| ORD ID | ord-68758d23a92b494db9df3b8bb3a8a64f |
| Source note | uspto-grants-2012_04 |