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4-Fluorophenyl sulfinate → 5-[(4-fluorophenyl)sulfonyl]-3-pyridinyl 2,3,4-tri-O-acetyl-5-thio-beta-D-xylopyranoside
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 4-Fluorophenyl sulfinate | HCID 4712689 | — |
| 反応物 | 5-iodo-3-pyridinyl 2,3,4-tri-O-acetyl-5-thio-beta-D-xylopyranoside | HCID 67291331 | — |
| 生成物 | 5-[(4-fluorophenyl)sulfonyl]-3-pyridinyl 2,3,4-tri-O-acetyl-5-thio-beta-D-xylopyranoside | HCID 67292581 | — |
反応手順
By following a procedure analogous to Example 139 starting from 5-iodo-3-pyridinyl 2,3,4-tri-O-acetyl-5-thio-β-D-xylopyranoside and 4-fluorophenyl sulfinate, 5-[(4-fluorophenyl)sulfonyl]-3-pyridinyl 2,3,4-tri-O-acetyl-5-thio-β-D-xylopyranoside is obtained in the form of a white solid (yield=24%).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08148407B2 |
| 出典データセット | uspto-grants-2012_04 |
| ORD ID | ord-d3edd9506b7a429e8958baee4a65c988 |
| 出典メモ | uspto-grants-2012_04 |