HuagongsheHuagongshe Chemistry Print Report · For research reference only
(4-(Piperidin-1-yl)phenyl)boronic acid → 6-[4-(1-piperidinyl)phenyl]-3-pyridinyl 2,3,4-tri-O-acetyl-5-thio-beta-D-xylo-pyranoside
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (4-(Piperidin-1-yl)phenyl)boronic acid | HCID 4192665 | — |
| Reactant | 6-bromo-3-pyridinyl 2,3,4-tri-O-acetyl-5-thio-beta-D-xylopyranoside | HCID 86625029 | — |
| Product | 6-[4-(1-piperidinyl)phenyl]-3-pyridinyl 2,3,4-tri-O-acetyl-5-thio-beta-D-xylo-pyranoside | HCID 67292540 | — |
Reaction Steps
By following a procedure analogous to Example 43 starting from [4-(1-piperidinyl)phenyl]boronic acid and 6-bromo-3-pyridinyl 2,3,4-tri-O-acetyl-5-thio-β-D-xylopyranoside, the expected compound is obtained in the form of a gray powder (yield=14%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08148407B2 |
| Source dataset | uspto-grants-2012_04 |
| ORD ID | ord-c347c10a6d50447a9b70ce8c6fc1fb0a |
| Source note | uspto-grants-2012_04 |