HuagongsheHuagongshe Chemistry Print Report · For research reference only
Formaldehyde → HCID 25017138, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Formaldehyde | HCID 712 | — |
| Reactant | Sodium triacetoxyborohydride | HCID 5049666 | — |
| Reactant | HCID 25017408 | HCID 25017408 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 25017138 | HCID 25017138 | — |
Reaction Steps
The compound of Example 27 (50 mg) was mixed with HCHO (2 eq, 37% in H2O), NaBH(OAc)3 (2 eq) in DCM (5 ml) and stirred at RT for 3 hours. The reaction was evaporated and purified with silica gel column to give the titled product (20 mg). Mass: (M+1), 476
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08148532B2 |
| Source dataset | uspto-grants-2012_04 |
| ORD ID | ord-d21c5d7bc9f34c82ac9e8d321a0f7697 |
| Source note | uspto-grants-2012_04 |