1,3-Benzodioxole-5-carbonyl chloride → N-(2-methylheptan-4-yl)benzo[d][1,3]dioxole-5-carboxamide

Participants

Reaction Steps

Prepared in a similar manner to example 1 using benzo[d][1,3]dioxole-5-carbonyl chloride and 2-methylheptan-4-amine (example 2a). 1H NMR (500 MHz, CDCl3): δ 0.93 (m, 9H); 1.38 (m, 5H); 1.53 (m, 1H); 1.66 (m, 1H); 4.21 (m, 1H); 5.61 (d, 1H); 6.01 (s, 2H); 6.82 (d, 1H); 7.26 (m, 2H). MS (278, M+H).

Provenance & Evidence