HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,3-Benzodioxole-5-carboxylic acid → (R)-methyl 2-(benzo[d][1,3]dioxole-6-carboxamido)-3-methylbutanoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,3-Benzodioxole-5-carboxylic acid | HCID 7196 | — |
| Reactant | (R)-methyl 2-amino-3-methylbutanoate | HCID 2305648 | — |
| Product | (R)-methyl 2-(benzo[d][1,3]dioxole-6-carboxamido)-3-methylbutanoate | HCID 57527948 | 50% |
Reaction Steps
Prepared in a similar manner to example 4 using benzo[d][1,3]dioxole-5-carboxylic acid and (R)-methyl 2-amino-3-methylbutanoate. Yield: 50%. MS (M+H, 280.1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08148536B2 |
| Source dataset | uspto-grants-2012_04 |
| ORD ID | ord-b81baeb36daa4e05aa5736b703d55155 |
| Source note | uspto-grants-2012_04 |