HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Bromopropane → 4-(N-(4-methoxybenzyl)-N-propylsulfamoyl)benzoic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Bromopropane | HCID 7840 | — |
| Reactant | Methyl 4-(N-(4-methoxybenzyl)sulfamoyl)benzoate | HCID 26527056 | — |
| Product | 4-(N-(4-methoxybenzyl)-N-propylsulfamoyl)benzoic acid | HCID 25205189 | — |
Reaction Steps
Prepared as in example 5-10 from Methyl 4-(N-(4-methoxybenzyl)sulfamoyl)benzoate (Example 5-10b) and n-propyl bromide. MS (M−H, 362.1); 1H NMR (400 MHz, CDCl3): δ, ppm: 0.70 (m, 3H), 1.35 (m, 3H), 3.08 (m, 2H), 3.73 (s, 3H), 4.31 (s, 2H), 6.83 (m, 2H), 7.17 (m, 2H), 7.93 (m, 2H), 8.23 (m, 2H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08148544B2 |
| Source dataset | uspto-grants-2012_04 |
| ORD ID | ord-3e5488646d95430a833dbb97936fe2e7 |
| Source note | uspto-grants-2012_04 |