HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-(Bromomethyl)-2,3-difluoro-benzene → HCID 57944952, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-(Bromomethyl)-2,3-difluoro-benzene | HCID 517984 | — |
| Reactant | Methyl 4-(N-(4-methoxybenzyl)sulfamoyl)benzoate | HCID 26527056 | — |
| Product | HCID 57944952 | HCID 57944952 | — |
Reaction Steps
Prepared as in example 5-10 from Methyl 4-(N-(4-methoxybenzyl)sulfamoyl)-benzoate (Example 5-10b) and 1-(bromomethyl)-2,3-difluorobenzene. 1H NMR (400 MHz, DMSO-d6): δ, ppm: 3.30 (s, 3H), 4.29 (s, 2H), 4.32 (s, 2H), 6.87 (d, 2H, J=8 Hz), 7.02-7.20 (m, 5H), 7.95 (d, 2H, J=8 Hz). 8.05 (d, 2H, J=8 Hz).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08148544B2 |
| Source dataset | uspto-grants-2012_04 |
| ORD ID | ord-c192b60fc79f42829fd4e6a0553ae3f4 |
| Source note | uspto-grants-2012_04 |