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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1687261Generated: October 29, 2026

HCID 67264286, compound → HCID 16744027, compound

https://huagongshe.com/reaction/1687261

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 67264286HCID 67264286—
CatalystPalladiumHCID 23938—
SolventEthanolHCID 702—
ProductHCID 16744027HCID 16744027—

Reaction Steps

1-(5-Methoxy-2-nitro-phenyl)-1H-pyrazole was treated under standard hydrogenation conditions (H2, EtOH, 10% Pd/C) to yield desired 4-Methoxy-2-pyrazol-1-yl-phenylamine as a crude solid, which was used for the subsequent reaction without further purification; TLC: 1:1 EtOAc/Hexane Rf 0.6, homogeneous; SM Rf 0.7; MS (m/e) 190.12 (M+H).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08148391B2
Source datasetuspto-grants-2012_04
ORD IDord-c086082835f740c0b821aa48b94fc068
Source noteuspto-grants-2012_04