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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1687273Generated: November 1, 2026

HCID 67263924, compound → HCID 67263595, compound

https://huagongshe.com/reaction/1687273

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 67263924HCID 67263924—
CatalystPalladiumHCID 23938—
SolventEthanolHCID 702—
ProductHCID 67263595HCID 67263595—

Reaction Steps

4-(4-Nitro-3-pyrazol-1-yl-phenyl)-morpholine was treated under standard hydrogenation conditions (H2, EtOH, 10% Pd/C) to yield desired 4-Morpholin-4-yl-2-pyrazol-1-yl-phenylamine as a crude oil, which was used for the subsequent reaction without further purification; TLC: 10:1 CH2Cl2:MeOH Rf 0.6, homogeneous (SM Rf 0.7); MS (m/e) 245.17 (M+H).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08148391B2
Source datasetuspto-grants-2012_04
ORD IDord-7e26b90ad17f45e4ad36ba149549f4ee
Source noteuspto-grants-2012_04