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HRID1687675

反应详情

EQUATION

反应方程式

HRID 1687675 的结构方程式

REACTANTS

反应物

2
结构：COC(=O)Cl
HCID6586

Methyl chlorocarbonate

C2H3ClO2

结构：CC1(C)CC(N)C(=O)Nc2cc([N+](=O)[O-])ccc21
HCID67264028

未命名化合物

PRODUCTS

生成物

1
结构：COC(=O)NC1CC(C)(C)c2ccc([N+](=O)[O-])cc2NC1=O
HCID67264643

未命名化合物

PROCEDURE

实验过程

(5,5-Dimethyl-8-nitro-2-oxo-2,3,4,5-tetrahydro-1H-1-benzazepin-3-yl)-carbamic acid methyl ester was prepared from 3-Amino-5,5-dimethyl-8-nitro-1,3,4,5-tetrahydro-1-benzazepin-2-one and Methyl chloroformate in an analogous manner to Example 1271d. Title compound is an off white solid. (94 mg, 38%) LCMS 308 (M+H).