4-Methylmorpholine → HCID 66841800, compound

Participants

Reaction Steps

To 1.05 g (4 mmole) of 2-chloro-4,6-di-(2-methoxyethoxy)-1,3,5-triazine (obtained as described in Example 1) in 3.5 mL of dry tetrahydrofuran was added 530 L of N-methyl morpholine. The solution was stirred for 30 minutes, filtered, and dried in an Abderhalden apparatus using acetone for 12 hours to yield 0.5 g (34%) of 4-(4,6-di-(2-methoxyethoxy)-1,3,5-triazin-2-yl)-4-methylmorpholinium chloride as a white powder. IR spectroscopy of the product (neat) identified the following characteristic IR absorption frequencies: 1605 cm−1, 1417 cm−1, 1336 cm−1, 1300 cm−1, 1118 cm−1, 1094 cm−1, 1068 cm−1, 1053 cm−1, 1028 cm−1, 1009 cm−1, 991 cm−1, 972 cm−1, 858 cm−1, and 821 cm−1.

Provenance & Evidence