Carbon tetrabromide → HCID 59201015, compound

Participants

Reaction Steps

A solution of (3-(4-(1,1,1,3,3,3-hexafluoro-2-(methoxymethoxy)propan-2-yl)-2-propylphenoxy)phenyl) methanol (1.09 g, 2.40 mmol) in methylene chloride (24 mL) was added with triphenylphosphine (0.95 g) and carbon tetrabromide (1.27 g) at 0° C. After completion of the reaction, the reaction solution was concentrated in vacuo. The obtained residue was purified using silica-gel column chromatography (hexane/ethyl acetate) and the title compound (1.04 g, yield 85%) was obtained as a colorless oil.

Provenance & Evidence