Water → HCID 59201074, compound

Participants

Reaction Steps

To a solution of 3-(4-(1,1,1,3,3,3-hexafluoro-2-(methoxymethoxy)propan-2-yl)-2-propylphenoxy)benz aldehyde (1.79 g, 3.97 mmol) in methanol, sodium borohydride (0.16 g) was added at 0° C. After completion of the reaction, the reaction solution was added with water, extracted with ethyl acetate, and then concentrated in vacuo. The obtained residue was purified using thin-layer silica-gel column chromatography (hexane/ethyl acetate) and the title compound (1.79 g, yield 100%) was obtained as a colorless oil.

Provenance & Evidence