Sodium Thiosulfate → HCID 59201144, compound

Participants

Reaction Steps

To a solution of 4-(1,1,1,3,3,3-hexafluoro-2-(methoxymethoxy)propan-2-yl)-2-propyl-1-(3-vinylphenoxy) benzene (686 mg, 1.52 mmol) in chloroform (10 mL), sodium hydrogen carbonate (510 mg), m-chloroperbenzoic acid (60%) (880 mg) were added at room temperature and the resultant mixture was stirred. After completion of the reaction, the reaction solution was added with an aqueous solution of sodium thiosulfate and a saturated aqueous solution of sodium hydrogen carbonate, extracted with ethyl acetate, and then concentrated in vacuo. The obtained residue was purified using silica-gel column chromatography (hexane/ethyl acetate) and the title compound (552 mg, yield 78%) was obtained as a colorless oil.

Provenance & Evidence