3-Chloroaniline → (3-Chloro-phenyl)-[2-(4-chloro-phenyl)-2H-indazol-3-yl]-amine

Participants

Reaction Steps

In analogy to the procedure described in example 4.1, 3-chloro-2-(4-chloro-phenyl)-2H-indazole (Ardakani, Manouchehr; Smalley, Robert K.; Smith, Richard H., Synthesis (1979), (4), 308-9) was reacted with 3-chloro-phenylamine ([108-42-9]) in N-methyl 2-pyrrolidone for 48 h at 175° C. in a sealed tube to give the title compound as off-white crystals. MS: m/e=354.2 [M+H+].

Provenance & Evidence