Back
HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1690604Generated: October 30, 2026

Lithium Hydroxide → HCID 45111769, compound

https://huagongshe.com/reaction/1690604

Reaction equation

Participants

RoleNameHCIDCharge
ReactantLithium HydroxideHCID 3939—
ReactantHCID 66905435HCID 66905435—
SolventiPrOAc brineHCID 131729614—
ProductHCID 45111769HCID 45111769—

Reaction Steps

In analogy to the procedure described in example 2.2, 3-chloro-4-[3-cyclohexyl-3-(2-phenyl-4,5,6,7-tetrahydro-2H-indazol-3-yl)-ureido]-benzoic acid methyl ester was treated with 1 N aqueous lithium hydroxide solution in THF/MeOH 1/1 for 1 h at ambient temperature to give the title compound as yellow solid. MS: m/e=493.3 [M+H+].

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08153663B2
Source datasetuspto-grants-2012_04
ORD IDord-9dc3c0e0088448cabb77fcc0303bb1f0
Source noteuspto-grants-2012_04