HuagongsheHuagongshe Chemistry Print Report · For research reference only
methyl 1-oxo-2,3-dihydro-1H-indene-5-carboxylate → 7-(4-Butylphenyl)-5,10-dihydroindeno[1,2-b]indole-2-carboxylic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | methyl 1-oxo-2,3-dihydro-1H-indene-5-carboxylate | HCID 10375253 | — |
| Reactant | HCID 66904838 | HCID 66904838 | — |
| Product | 7-(4-Butylphenyl)-5,10-dihydroindeno[1,2-b]indole-2-carboxylic acid | HCID 16046754 | — |
Reaction Steps
By reacting (4′-Butyl-biphenyl-3-yl)-hydrazine hydrochloride (example 70, step 1) and 1-oxo-indan-5-carboxylic acid methyl ester as described in example 1 followed by hydrolysis as described in example 2 the title material is obtained in similar yield. ESMS m/z 382.1 (M+H+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08153671B2 |
| Source dataset | uspto-grants-2012_04 |
| ORD ID | ord-68e559a41c104bf3be629e28ccc6e29a |
| Source note | uspto-grants-2012_04 |