HuagongsheHuagongshe Chemistry Print Report · For research reference only
6-Nitroquinolin-5-ylamine → Quinoline-5,6-diamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 6-Nitroquinolin-5-ylamine | HCID 118901 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | Quinoline-5,6-diamine | HCID 426874 | — |
Reaction Steps
A mixture of 5-Amino-6-nitroquinoline (650 mg, 3.44 mmol), Pd/C (70 mg) and 15 mL of EtOH was stirred under H2 (balloon) overnight. The reaction mixture was filtered through Celite and the filtrate was concentrated to give 5,6-diaminoquinoline.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08153626B2 |
| Source dataset | uspto-grants-2012_04 |
| ORD ID | ord-291f51b0392641508c6389841d1f93e1 |
| Source note | uspto-grants-2012_04 |