HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → Ethyl 5-[(3,5-dinitropyridin-2-yl)amino]pentanoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | 2-Chloro-3,5-dinitropyridine | HCID 75738 | — |
| Reactant | ETHYL 5-AMINOVALERATE | HCID 11469139 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | Ethyl 5-[(3,5-dinitropyridin-2-yl)amino]pentanoate | HCID 86643267 | 76% |
Reaction Steps
A procedure similar to that of the method described in step C.1 is carried out, starting from 1.2 g (5.9 mmol) of 2-chloro-3,5-dinitropyridine, 1.03 g (7.07 mmol) of ethyl 5-aminovalerate and 0.9 g (8.84 mmol) of triethylamine in 20 ml of dioxane. This gives 1.4 g of expected product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08153796B2 |
| Source dataset | uspto-grants-2012_04 |
| ORD ID | ord-848cf88c531d449cbac9a4d000590495 |
| Source note | uspto-grants-2012_04 |