HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-methylpiperidine-4-carboxamide → HCID 44545153, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-methylpiperidine-4-carboxamide | HCID 2760460 | — |
| Reactant | HCID 66909826 | HCID 66909826 | — |
| Product | HCID 44545153 | HCID 44545153 | — |
Reaction Steps
3-(2-(2-(Tert-butoxycarbonylamino)pyrimidin-5-yl)-6-morpholino-9H-purin-9-yl)propanoic acid (50 mg) was reacted with N-methylpiperidine-4-carboxamide via General Procedure F followed by Boc deprotection via General Procedure E to give 10.9 mg 111 as white solid following reverse phase purification. MS (Q1) 495.3 (M)+
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08158624B2 |
| Source dataset | uspto-grants-2012_04 |
| ORD ID | ord-3d7f5ba8aae74565b0bea6a47fa74aeb |
| Source note | uspto-grants-2012_04 |