HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-(4,4,5,5-Tetramethyl-1,3,2-dioxaborolan-2-yl)pyridin-2-amine → HCID 44543765, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-(4,4,5,5-Tetramethyl-1,3,2-dioxaborolan-2-yl)pyridin-2-amine | HCID 2756555 | — |
| Reactant | 2-Chloro-9-methyl-6-(4-morpholinyl)-9H-purine | HCID 71500687 | — |
| Product | HCID 44543765 | HCID 44543765 | — |
Reaction Steps
4-(2-Chloro-9-methyl-9H-purin-6-yl)morpholine (20 mg) was reacted with 5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)pyridin-2-amine via General Procedure A and purified via reverse phase HPLC to give 9.3 mg of 128 as a white solid. MS (Q1) 312.3 (M)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08158624B2 |
| Source dataset | uspto-grants-2012_04 |
| ORD ID | ord-e04259e047884bb3b4b53d2267c5fc43 |
| Source note | uspto-grants-2012_04 |