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HRID1692682

反应详情

EQUATION

反应方程式

HRID 1692682 的结构方程式

REACTANTS

反应物

2
结构：CC1(C)OB(c2cccc3[nH]ncc23)OC1(C)C
HCID45480186

4-(4,4,5,5-Tetramethyl-1,3,2-dioxaborolan-2-yl)-1H-indazole

C13H17BN2O2

结构：Cn1c(C(C)(C)O)nc2c(N3CCOCC3)nc(Cl)nc21
HCID58015213

未命名化合物

PRODUCTS

生成物

1
结构：Cn1c(C(C)(C)O)nc2c(N3CCOCC3)nc(-c3cccc4[nH]ncc34)nc21
HCID44543769

未命名化合物

PROCEDURE

实验过程

Crude 2-(2-chloro-9-methyl-6-morpholino-9H-purin-8-yl)propan-2-ol was reacted with 4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1H-indazole via Procedure A and purified via reverse phase HPLC to give 56.6 mg of 132 as a white solid. MS (Q1) 394.3 (M)+

WORKUP

后处理

  1. custompurified via reverse phase HPLC