反应详情

温度

120 °C

A pressure tube, equipped with a magnetic stirring bar, was charged with Compound 2 (0.54 g, 3 mmole) and 1,3-diiodopropane (2.66 g, 9 mmole). The mixture was heated to ˜120° C. for 3 hours. The residue was extensively washed with ethyl acetate and diethyl ether and dried under vacuum to give 0.4 g of yellow solid Compound 3 (yield ˜28%).

1. customA pressure tube, equipped with a magnetic stirring bar
2. washThe residue was extensively washed with ethyl acetate and diethyl ether
3. customdried under vacuum