HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Fluoro-3-methylbenzo[b]thiophene-2-sulphonyl chloride → HCID 59759972, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Fluoro-3-methylbenzo[b]thiophene-2-sulphonyl chloride | HCID 2774586 | — |
| Reactant | HCID 54351109 | HCID 54351109 | — |
| Product | HCID 59759972 | HCID 59759972 | 70.5% |
Reaction Steps
This compound was prepared in analogy to Example 1 starting from 4-bromo-2-methylsulfanylmethyl-phenylamine (Allen, David George; Eldred, Colin David; Judkins, Brian David; Mitchell, William Leonard, WO 9749699, 4.6 g) and 5-fluoro-3-methylbenzo[b]thiophene-2-sulphonyl chloride (1.06 g) to obtain the desired compound (1.3 g) as a brownish solid. MS (ISN): 458.1, 460.0 (M−H)−
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08158655B2 |
| Source dataset | uspto-grants-2012_04 |
| ORD ID | ord-31d899b72fc3444f84bb9199aa81263a |
| Source note | uspto-grants-2012_04 |