Hydrochloric Acid → HCID 59759965, compound

Participants

Reaction Steps

To a solution of benzyl-(2-methanesulfonyl-4-pyridin-4-yl-phenyl)-amine (2.0 g) in dioxane/methanol 1:1 (100 ml) was added 2N HCl (5 ml) and palladium black (1.0 g). The reaction mixture was hydrogenated at 1.1 bar and rt for 18 h. The catalyst was filtered off over a microfilter and washed with methanol. The filtrate was evaporated to dryness to obtain the desired compound (1.45 g) as a yellowish solid. MS (ISP): 249.1 (M+H)+

Provenance & Evidence