HRID1693121

反应详情

EQUATION

反应方程式

REACTANTS

反应物

结构：Cc1c(S(=O)(=O)Nc2ccc(C3CCNCC3)cc2S(C)(=O)=O)sc2ccc(F)cc12.Cl

HCID24966321

未命名化合物

PRODUCTS

生成物

结构：Cc1c(S(=O)(=O)Nc2ccc(C3CCNCC3)cc2S(C)(=O)=O)sc2ccc(F)cc12

HCID24966322

未命名化合物

收率 0%

AUXILIARIES

试剂、催化剂与溶剂

溶剂HCID86621318

未命名化合物

PROCEDURE

实验过程

5-Fluoro-3-methyl-benzo[b]thiophene-2-sulfonic acid(2-methanesulfonyl-4-piperidin-4-yl-phenyl)-amide hydrochloride (cf. Example 20 g, 6 mg) was run through an HPLC-column with acetonitrile/water/formic acid to obtain the title compound (3 mg) as an off-white foam. MS (ISP): 483.3 (M+H)+