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HRID1693470

反应详情

EQUATION

反应方程式

HRID 1693470 的结构方程式

REACTANTS

反应物

2
结构：COCCOC1CCNCC1.Cl
HCID22061354

未命名化合物

结构：O=C(N[C@@H](Cc1ccc(F)cc1)C(=O)O)c1cc2cc(Cl)ncc2[nH]1
HCID59753699

未命名化合物

PRODUCTS

生成物

1
结构：COCCOC1CCN(C(=O)[C@H](Cc2ccc(F)cc2)NC(=O)c2cc3cc(Cl)ncc3[nH]2)CC1
HCID59753570

未命名化合物

PROCEDURE

实验过程

The title compound was prepared according to EXAMPLE 229 from 2-(S)-[(5-chloro-1H-pyrrolo[2,3-c]pyridine-2-carbonyl)amino]-3-(4-fluorophenyl)propionic acid (EXAMPLE 228) and 4-(2-methoxyethoxy)piperidine hydrochloride (Preparation 82). Purification by chromatography using dichloromethane/methanol (95:5) as the eluent gave the title compound as an off-white powder. m/z (ES+) 503.26 [M+H]+; RT=3.3 min.

WORKUP

后处理

  1. customThe title compound was prepared
  2. customPurification by chromatography