HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzyl Isothiocyanate → 4-Benzyl-2-diphenylmethyl-1,2,4-thiadiazolidine-3,5-dione
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzyl Isothiocyanate | HCID 2346 | — |
| Reactant | Diethyl Ether | HCID 3283 | — |
| Reactant | (Isocyanatomethylene)dibenzene | HCID 4250935 | — |
| Product | 4-Benzyl-2-diphenylmethyl-1,2,4-thiadiazolidine-3,5-dione | HCID 11574332 | — |
Reaction Steps
Reagents: Benzylisothiocyanate (6.5 mmol, 0.85 mL), diphenylmethyl-isocyanate (6.5 mmol, 1.23 mL) and SO2Cl2 (6.5 mmol, 0.52 mL) in diethyl ether (25 mL). Isolation: filtration of reaction mixture. Purification: recrystallization from MeOH.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08158661B2 |
| Source dataset | uspto-grants-2012_04 |
| ORD ID | ord-c37890a10c3f4f14aa2fae4b74d500dc |
| Source note | uspto-grants-2012_04 |