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5-Cyclohex-1-enyl-3-phenylamino-thiophene-2-carboxylic acid methyl ester → HCID 178499262、化合物
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 5-Cyclohex-1-enyl-3-phenylamino-thiophene-2-carboxylic acid methyl ester | HCID 57795360 | — |
| 反応物 | HCID 178461265 | HCID 178461265 | — |
| 生成物 | HCID 178499262 | HCID 178499262 | 27% |
反応手順
The methyl ester from Step I (565 mg, 1.13 mmol) was acylated with trans-4-methylcyclohexyl carboxylic acid chloride as previously described (example 11, step II) to give 41 mg (27%) of 5-cyclohex-1-enyl-3-[(trans-4-methyl-cyclohexanecarbonyl)-phenyl-amino]-thiophene-2-carboxylic acid methyl ester.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08158675B2 |
| 出典データセット | uspto-grants-2012_04 |
| ORD ID | ord-01fd56d0e4fe477e9fbb8646bd63e232 |
| 出典メモ | uspto-grants-2012_04 |