(5-Chloro-2-hydroxyphenyl)boronic Acid (contains varying amounts of Anhydride) → HCID 67280610, compound

HRID 1694719Notes

Reaction equation

HRID 1694719 reaction equation
Br[C:2]1[CH:3]=[N:4][C:5]([N:8]([CH2:13][C:14]2[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=2)[S:9]([CH3:12])(=[O:11])=[O:10])=[N:6][CH:7]=1.[Cl:20][C:21]1[CH:22]=[CH:23][C:24]([OH:30])=[C:25](B(O)O)[CH:26]=1>>[Cl:20][C:21]1[CH:26]=[CH:25][C:24]([OH:30])=[C:23]([C:2]2[CH:3]=[N:4][C:5]([N:8]([CH2:13][C:14]3[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=3)[S:9]([CH3:12])(=[O:11])=[O:10])=[N:6][CH:7]=2)[CH:22]=1

Participants

3

Reactant 2

HCID 23005362(5-Chloro-2-hydroxyphenyl)boronic Acid (contains varying amounts of Anhydride)HCID 67281141HCID 67281141, compound

Product 1

HCID 67280610HCID 67280610, compound

Procedure

The subtitle compound was prepared by the method of example 1 step (ii) using the product from step (i) and 5-chloro-2-hydroxyphenyl-boronic acid, yield 0.25 g.

Sources & evidence

ORD record
ord-e8720421b47b48fe9ad2476d87f27ac6
Source dataset
uspto-grants-2012_04
Patent number
US08158820B2

Reaction notes

Loading…