(5-Chloro-2-hydroxyphenyl)boronic Acid (contains varying amounts of Anhydride) → HCID 67280875, compound

HRID 1694721Notes

Reaction equation

HRID 1694721 reaction equation
Br[C:2]1[CH:3]=[N:4][C:5]([N:8]([CH2:14][C:15]2[CH:20]=[CH:19][CH:18]=[CH:17][CH:16]=2)[S:9]([CH2:12][CH3:13])(=[O:11])=[O:10])=[N:6][CH:7]=1.[Cl:21][C:22]1[CH:23]=[CH:24][C:25]([OH:31])=[C:26](B(O)O)[CH:27]=1>>[Cl:21][C:22]1[CH:27]=[CH:26][C:25]([OH:31])=[C:24]([C:2]2[CH:3]=[N:4][C:5]([N:8]([CH2:14][C:15]3[CH:20]=[CH:19][CH:18]=[CH:17][CH:16]=3)[S:9]([CH2:12][CH3:13])(=[O:11])=[O:10])=[N:6][CH:7]=2)[CH:23]=1

Participants

3

Reactant 2

HCID 23005362(5-Chloro-2-hydroxyphenyl)boronic Acid (contains varying amounts of Anhydride)HCID 67280503HCID 67280503, compound

Product 1

HCID 67280875HCID 67280875, compound

Procedure

The subtitle compound was prepared by the method of example 1 step (ii) using the product from step (i) and 5-chloro-2-hydroxyphenyl-boronic acid, yield 0.25 g.

Sources & evidence

ORD record
ord-47aba24de5bf4b99a5b1b4e061368b35
Source dataset
uspto-grants-2012_04
Patent number
US08158820B2

Reaction notes

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