3-Iodobenzonitrile → HCID 67280513, compound

HRID 1694765Notes

Reaction equation

I[C:2]1[CH:3]=[C:4]([CH:7]=[CH:8][CH:9]=1)[C:5]#[N:6].[Cl:10][C:11]1[CH:12]=[CH:13][C:14]([O:20][CH3:21])=[C:15](B(O)O)[CH:16]=1>>[Cl:10][C:11]1[CH:16]=[CH:15][C:14]([O:20][CH3:21])=[C:13]([C:2]2[CH:9]=[CH:8][CH:7]=[C:4]([C:5]#[N:6])[CH:3]=2)[CH:12]=1

Participants

Reactant 2

HCID 1443413-Iodobenzonitrile

HCID 27357515-Chloro-2-methoxyphenylboronic acid

Product 1

HCID 67280513HCID 67280513, compound

Procedure

The subtitle compound was prepared by the method of example 1 step (ii) using 3-iodobenzonitrile and 5-chloro-2-methoxyphenyl boronic acid. Yield 0.465 g

Sources & evidence

ORD record: ord-75d92960393440af8bd3587bdcf8ea46
Source dataset: uspto-grants-2012_04
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US08158820B2

Reaction notes

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