Hydrazine, propyl- → HCID 58951959, compound

HRID 1694818Notes

Reaction equation

HRID 1694818 reaction equation
[CH2:1]([N:8]1[C:12]([CH2:13][CH:14]([C:19](=O)[CH2:20][CH3:21])[C:15](=O)[CH2:16][CH3:17])=[CH:11][N:10]=[CH:9]1)[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[CH2:23]([NH:26][NH2:27])[CH2:24][CH3:25]>>[CH2:1]([N:8]1[C:12]([CH2:13][C:14]2[C:19]([CH2:20][CH3:21])=[N:27][N:26]([CH2:23][CH2:24][CH3:25])[C:15]=2[CH2:16][CH3:17])=[CH:11][N:10]=[CH:9]1)[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1

Participants

3

Reactant 2

HCID 42007Hydrazine, propyl-HCID 58951913HCID 58951913, compound

Product 1

HCID 58951959HCID 58951959, compound

Procedure

4-(3-Benzyl-3H-imidazol-4-ylmethyl)-3,5-diethyl-1-propyl-1H-pyrazole was prepared from 4-(3-benzyl-3H-imidazol-4-ylmethyl)-heptane-3,5-dione and propylhydrazine in analogy to Example 55 b): off-white solid; MS (ISP): 337.1 ((M+H)+.).

Sources & evidence

ORD record
ord-c81906d2f40049f6b44d113859502307
Source dataset
uspto-grants-2012_04
Patent number
US08158668B2

Reaction notes

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