反应详情

温度

20 °C

Morpholine (1.1 ml) was added to a solution of [4-bromo-2-(trifluoromethyl)phenyl]sulfonyl chloride (2.03 g) in DCM (7 ml) at 0° C. and stirred at 20° C. for 16 h. Water was added and the mixture was extracted with DCM. The organic extracts were dried (MgSO4), evaporated and purified by chromatography (silica, petrol—ether as to eluent) to give the sub-title compound 2.10 g).

1. extractionthe mixture was extracted with DCM
2. dry with materialThe organic extracts were dried (MgSO4)
3. customevaporated
4. custompurified by chromatography (silica, petrol—ether as to eluent)