HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl 2-ethylbenzoate → 3-(2-Ethyl-phenyl)-3-oxo-propionitrile
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl 2-ethylbenzoate | HCID 583295 | — |
| Reactant | HCID 178418806 | HCID 178418806 | — |
| Product | 3-(2-Ethyl-phenyl)-3-oxo-propionitrile | HCID 20387509 | 92% |
Reaction Steps
The product was prepared according to the general procedure for aminopyrazole synthesis (route A1) from 2-ethyl-benzoic acid methyl ester (2.9 g, 17.6 mmol, 1.0 eq). The crude product was extracted with DCM as a yellow oil and used in the following step without further purification (2.8 g, yield: 92%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08163729B2 |
| Source dataset | uspto-grants-2012_04 |
| ORD ID | ord-cca74df93a524a5280b2da09963a1513 |
| Source note | uspto-grants-2012_04 |