HCID 67187037, compound → HCID 67274088, compound

HRID 1695184Notes

Reaction equation

HRID 1695184 reaction equation
[NH2:1][C:2]1[CH:6]=CNN=1.CO[C:9](=[O:22])[C:10]1[CH:15]=[CH:14][C:13]([O:16][CH2:17][CH:18]2[CH2:20][CH2:19]2)=[CH:12][C:11]=1[CH3:21]>>[CH:18]1([CH2:17][O:16][C:13]2[CH:14]=[CH:15][C:10]([C:9](=[O:22])[CH2:6][C:2]#[N:1])=[C:11]([CH3:21])[CH:12]=2)[CH2:19][CH2:20]1

Participants

3

Reactant 2

HCID 67187037HCID 67187037, compoundHCID 178418806HCID 178418806, compound

Product 1

HCID 67274088HCID 67274088, compoundYield 69%

Procedure

The product was prepared according to the general procedure for aminopyrazole synthesis from 4-cyclopropylmethoxy-2-methyl-benzoic acid methyl ester (route Albis). 0.54 g of the title product was extracted from water and dried (yield 69%) and used directly for the next step.

Workup

  1. customThe product was prepared
  2. extraction0.54 g of the title product was extracted from water
  3. customdried (yield 69%)

Sources & evidence

ORD record
ord-a863990f5c894b4f822bb200ff99b8f3
Source dataset
uspto-grants-2012_04
Patent number
US08163729B2

Reaction notes

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