HCID 7018382, compound → HCID 24691440, compound

HRID 1695246Notes

Reaction equation

HRID 1695246 reaction equation
[NH2:1][C:2]1[CH:6]=CNN=1.CO[C:9](=[O:20])[C:10]1[CH:15]=[CH:14][CH:13]=[CH:12][C:11]=1[O:16][CH:17]([F:19])[F:18]>>[F:19][CH:17]([F:18])[O:16][C:11]1[CH:12]=[CH:13][CH:14]=[CH:15][C:10]=1[C:9](=[O:20])[CH2:6][C:2]#[N:1]

Participants

3

Reactant 2

HCID 7018382HCID 7018382, compoundHCID 178418806HCID 178418806, compound

Product 1

HCID 24691440HCID 24691440, compound

Procedure

The product was prepared according to the general procedure for aminopyrazole synthesis from 1.5 g (7.4 mmol, 1.0 eq) of 2-Difluoromethoxy-benzoic acid methyl ester (route A1bis). The crude product was used directly for the next step.

Workup

  1. customThe product was prepared

Sources & evidence

ORD record
ord-0f15433e20a74235b1d0fedbee0f400f
Source dataset
uspto-grants-2012_04
Patent number
US08163729B2

Reaction notes

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