HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium borohydride → HCID 21921167, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium borohydride | HCID 4311764 | — |
| Reactant | N-(5-Acetyl-indan-2-YL)-4-fluoro-benzamide | HCID 21920974 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 21921167 | HCID 21921167 | — |
Reaction Steps
400 mg (1.35 mmol) N-(5-acetyl-indan-2-yl)-4-fluoro-benzamide were dissolved in 10 ml of methanol, then 100 mg (2.7 mmol) sodium borohydride were added. The mixture was worked up by dropping onto ice/HCl, the resulting solid was filtered off.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08163751B2 |
| Source dataset | uspto-grants-2012_04 |
| ORD ID | ord-51d7265b3dcf4f578852d6ad6333a988 |
| Source note | uspto-grants-2012_04 |