Chloroacetyl chloride → HCID 178520795, compound

Participants

Reaction Steps

Prepared from rac-N2-(5-fluoro-indan-1-yl)-4H-benzo[d][1,3]oxazine-2,6-diamine (Example 11) (300 mg, 1.01 mmol) and chloroacetyl chloride (85 ul, 1.06 mmol) according to the procedure described for Example 3 step A. Obtained the title compound as a light brown foam (370 mg, 98%), MS (ISP) m/e=374.2 [(M+H)+] and 376 [(M+2+H)+].

Provenance & Evidence