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HRID1695640

反应详情

EQUATION

反应方程式

HRID 1695640 的结构方程式

REACTANTS

反应物

2
结构：Cc1ccc(CN)o1
HCID2724683

5-Methylfurfurylamine

C6H9NO

结构：CC(C)(C)[Si](C)(C)OCc1cc([N+](=O)[O-])ccc1N=C=S
HCID46855450

未命名化合物

PRODUCTS

生成物

1
结构：Cc1ccc(CNC2=Nc3ccc([N+](=O)[O-])cc3CO2)o1
HCID178425507

未命名化合物

收率 79.1%

PROCEDURE

实验过程

Prepared from tert-butyl-(2-isothiocyanato-5-nitro-benzyloxy)-dimethyl-silane (Example C1) (2.0 g, 6.16 mmol; HPLC: 4.446 min) and 5-methyl-2-furanmethanamine (CAS 14003-16-8) (0.685 g, 6.163 mmol) according to the procedure described for Example 1. Obtained the title compound as a yellow solid (1.40 g, 79%, HPLC 1.624 min), MS (ISP) m/e=326.2 [(M+H)+].