HuagongsheHuagongshe Chemistry Print Report · For research reference only
Morpholine → HCID 178425506, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Morpholine | HCID 8083 | — |
| Reactant | HCID 178425504 | HCID 178425504 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 178425506 | HCID 178425506 | 87% |
Reaction Steps
Prepared from the above described 2-chloro-N-{2-[(5-methyl-furan-2-ylmethyl)-amino]-4H-benzo[d][1,3]oxazin-6-yl}-acetamide (100 mg, 0.300 mmol) and morpholine (0.260 ml 2.996 mmol) in acetonitrile (1 ml) according to the procedure described for Example 3 step B. Obtained the title compound as a white solid (100 mg, 87%), MS (ISP) m/e=385.3 [(M+H)+].
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08163740B2 |
| Source dataset | uspto-grants-2012_04 |
| ORD ID | ord-fcec6a8402d341168bc462ba0264bc0b |
| Source note | uspto-grants-2012_04 |