HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cyclopropanesulfonyl chloride → HCID 178527453, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cyclopropanesulfonyl chloride | HCID 2760919 | — |
| Reactant | HCID 178507250 | HCID 178507250 | — |
| Product | HCID 178527453 | HCID 178527453 | 2.5% |
Reaction Steps
Prepared from N2-cycloheptyl-4H-benzo[d][1,3]oxazine-2,6-diamine (example 92) (200 mg, 0.77 mmol) and cyclopropylsulfonyl chloride (119 mg, 0.85 mmol) according to the procedure described for example 27. Obtained the title compound as a white solid (7 mg, 2.5%), MS (ISP) m/e=364.3 [(M+H)+].
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08163740B2 |
| Source dataset | uspto-grants-2012_04 |
| ORD ID | ord-f0b437e47ad04da183ea5838cc81a1bc |
| Source note | uspto-grants-2012_04 |