Cyclopropanesulfonyl chloride → HCID 178527455, compound

Participants

Reaction Steps

Prepared from the above described N2-(2-phenoxy-ethyl)-4H-benzo[d][1,3]oxazine-2,6-diamine (155 mg, 0.50 mmol, HPLC 0.691 min) and cyclopropanesulfonyl chloride (77 mg, 0.55 mmol) according to the procedure described for Example 27. Obtained the title compound as an off-white foam (140 mg, 73%, HPLC 1.261 min), MS (ISP) m/e=388.3 [(M+H)+].

Provenance & Evidence